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By S. Ted Oyama and Joe W. Hightower (Eds.)

ISBN-10: 0841213798

ISBN-13: 9780841213791

ISBN-10: 0841226377

ISBN-13: 9780841226371

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Soc. A. 1969, 1066. 30. Rappé, A. ; Goddard, W. A. J. Amer. Chem. Soc. 1982, 104, 3287. 31. Thesefreeenergies were calculatedfromthe data presented in ref. 30, and from tabulations in O'Neal, H. ; Benson, S. W. "Thermochemistry of Free Radicals" in Free Radicals, Kochi, J. K. ; p. 275, Wiley, New York, 1973, and in Perry's Chemical Engineering Handbook, Sixth Edition, Perry, R. ; Green, D. ; Maloney, J. O. 3-147, McGraw-Hill, New York, 1984. The free energy of hydration of Cl CrO to Cl CrO(OH) was estimated by correlating bond dissociation and heat of formation data for a series of compounds tofreeenergies reported in ref.

To s t u d y t h e e f f e c t o f l o a d i n g , v a r i o u s amounts o f v a n a d i a were d e p o s i t e d on t h e t i t a n i a s u p p o r t . The Raman spectra of t i t a n i a supported vanadia catalysts as a f u n c t i o n o f vanadia loading reveal t h e presence o f three different vanadia s p e c i e s on t h e T i 0 support under dehydration c o n d i t i o n s a s shown i n F i g u r e 2. A t low l o a d i n g s ( — 1% V 0 ) , a s i n g l e s h a r p band i s p r e s e n t a t — 1 0 2 7 cm" w h i c h i s a s s i g n e d t o an i s o l a t e d t e t r a h e d r a l coordinated s u r f a c e vanadium oxide species containing one t e r m i n a l V=0 bond and t h r e e b r i d g i n g V - 0 - T i bonds [19] .

8. ; Kubokawa, Y. J. Phys. Chem. 1980, 84, 3440. ; Busca, G. J. Catal. 1991, 116, 586. 9. ; Wachs, I. E. J. Phys. Chem. 1989, 93, 6796. ; Wachs, I. , unpublished results. 10. ; Wachs, I. , in preparation. 11. Vuurman, Μ. ; Wachs, I. ; Oskam, A. J. Mol. , 1992, in press. 12. Kim, D. ; Wachs, I. E. J. Catal. 1992, in press. 13. (a) Wainwright, M. ; Foster, N. R. Catal. Rev. 1979, 19, 211. ; Raveling, H. Ber. Bunsenges. phy. Chem. 1980, 84, 912. 14. ; Abadzhijeva, N. React. Kinet. Catal. Lett. 1975, 2, 431.

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Catalytic Selective Oxidation by S. Ted Oyama and Joe W. Hightower (Eds.)


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